ASTM D6730 DANI Optimized Method with Cryo

Oven

• Initial temperature 5 °C
• Initial time 10 min
• First program rate 5 °C/min
• First hold temperature 50 °C
• First hold time 0 min
• Second program rate 1.5 °C/min
• Final temperature 200 °C
• Final hold time 5 min

Injector

• Temperature 250 °C
• Split ratio 150:1
• Sample size 0.5 uL

Detector

• FID
• Temperature 250 °C
• Hydrogen 30 mL/min
• Air 300 mL/min
• Nitrogen 30 mL/min

Carrier gas

• Helium, pressure constant: 4.16 bar