ASTM D6730

Oven

• Linear carrier flow (He) 2.4 ml/min
• Initial temperature 35 °C
• First hold temperature 5 °C
• First hold time 10 min
• First program rate 5 °C/min
• Second temperature ≈ 49
• Second hold time ≈ 55
• Second program rate 1.6 °C/min
• Final temperature 200 °C
• Final hold time 5 min
• Analysis time ≈ 170

Injector

• Temperature 250 °C
• Split ratio 100:1
• Sample size 0.1 - 0.2 uL

Detector

• FID
• Temperature 250 °C
• Hydrogen flow 35 mL/min
• Air flow 350 mL/min
• Make up flow He 20 mL/min

Carrier gas

• Helium
• EPC pressure 301 kPa
• Linear velocity 28 cm/s
• Gas saver flow 25
• Gas saver time 2